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0542 - 有機化學實驗 Organic Chemistry Lab


教育目標 Course Target

導引學生如何完成有機化學反應,終止反應操作,包括淬取及快速管柱層析,進而得到產物。使學生學習正確的實驗邏輯觀念,從失敗的實驗找出問題,進一步克服困難。再與課堂上教授的反應進一步與實驗結合,讓學生能學以應用。1.Crystallization 2.Extraction(acid / base extraction) 3.Chromatography(Thin-Layer and Column Chromatography) 4.Conversion of Alcohols to Halides(Preparation of n-Butyl Bromide) 5.Williamson Ether Synthesis(Preparation of n-Butyl Methyl Ether) 6.Resolution of racemic phenylsuccinic acidusing(-)Proline as a resolving agent 7.Conversion of Alcohols to Alkenes(Preparation of Cyclohexene) 8.Nitration of Methyl Benzoate 9.Aldehydes and Ketones 10.Fries Rearrangement Accelerated by Microwave RadiationGuide students on how to complete organic chemical reactions, terminate reaction operations, including quenching and fast column chromatography, and obtain products. Enable students to learn correct experimental logical concepts, identify problems from failed experiments, and further overcome difficulties. It is then further combined with the professor’s reaction in class and experiments so that students can apply what they have learned. 1.Crystallization 2.Extraction (acid / base extraction) 3.Chromatography (Thin-Layer and Column Chromatography) 4.Conversion of Alcohols to Halides (Preparation of n-Butyl Bromide) 5.Williamson Ether Synthesis (Preparation of n-Butyl Methyl Ether) 6.Resolution of racemic phenylsuccinic acidusing(-)Proline as a resolving agent 7.Conversion of Alcohols to Alkenes (Preparation of Cyclohexene) 8.Nitration of Methyl Benzoate 9.Aldehydes and Ketones 10.Fries Rearrangement Accelerated by Microwave Radiation


課程概述 Course Description

有機化學實驗的目在於訓練學生利用實驗操作、現象觀察、化合物的製備、分離純化到鑑定的過程,經過思考、總結及歸納形成對有機化學反應、化合物的性質、結構產生一定程度的相關知識,並使這些知識能與課本理論相互呼應、驗證、結合,透過實驗反覆練習,來增進學生手、眼、心合一,加深對有機化學課程的興趣及了解。
The purpose of the organic chemistry experiment is to train students to use the process of experimental operations, phenomenon observation, preparation of compounds, separation, purification and identification, and through thinking, summary and induction to form a certain degree of relevant knowledge about organic chemical reactions, properties and structures of compounds. This knowledge can be echoed, verified, and combined with textbook theories. Through repeated experiments and practice, students can improve the integration of hands, eyes, and minds, and deepen their interest in and understanding of organic chemistry courses.


參考書目 Reference Books

L. F. Fieser and K. Williamson , Organic Experiment
l. F. Fieser and K. Williamson, organic experiment


評分方式 Grading

評分項目 Grading Method 配分比例 Grading percentage 說明 Description
平時成績平時成績
usual results
35
期中考試期中考試
midterm exam
15
報告成績報告成績
Report results
35
期末考試期末考試
final exam
15

授課大綱 Course Plan

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Course Information

Description

學分 Credit:1-1
上課時間 Course Time:Tuesday/5,6,7[BS603]
授課教師 Teacher:張源杰
修課班級 Class:化學系化學組2
選課備註 Memo:限人工加選,開學第一週實驗安全教育訓練未參加者不得選課。
授課大綱 Course Plan: Open

選課狀態 Attendance

There're now 44 person in the class.
目前選課人數為 44 人。

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